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Description
Phenyl-2-nitropropene is a chemical compound with the chemical formula is C9H9NO2. It can be produced by the reaction of benzaldehyde and nitroethane in the presence of a basic catalyst. In this reaction, the base deprotonates nitroethane to form a resonance stabilized anion. This anion nucleophilically adds to the aldehyde forming a beta nitro alcohol, which is subsequently dehydrated to yield the nitroalkene. This reaction is known as a nitroaldol reaction. Phenyl-2-nitropropene can be reduced in the presence of a catalyst to produce phenylacetone, which is a controlled precursor of methamphetamine. However, with lithium aluminium hydride it can simply be reduced to directly form amphetamine in moderate yields.
Synthesis of phenyl-2-nitropropene
CAS No.:                                                                     2904209090
Other Names:                                                             2-nitro-1-phenyl-1-propene
MF:                                                                              C9H9NO2
Molecular Weight:                                                     163.17300
PSA                                                                              45.82000
LOGP                                                                              2.84730
Density                                                                           1.141 g/cm3
Melting point:                                                             63-65ºC
Boiling point                                                                  263ºC at 760 mmHg
Sample:                                                                        Availiable